HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonyl azide → HCID 86735459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonyl azide | HCID 13661 | — |
| Reactant | HCID 13350949 | HCID 13350949 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 86735459 | HCID 86735459 | 87% |
Reaction Steps
In accordance with the process of Example 2, (Z)-3-oxo-6-octenoic acid methyl ester (0.77 g; 4.52 m mol), triethylamine (0.46 g; 4.52 m mol), p-toluenesulfonylazide (0.89 g; 4.52 m mol) were used as starting materials to obtain 0.77 g of (Z)-2-diazo-3-oxo-6-octenoic acid methyl ester as yellow oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04073799 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-fb843b45d29445c2945926bf0a02b601 |
| Source note | uspto-grants-1978_02 |