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3-Chloropropyl(diethyl)amine → 1-Propanamine, N,N-diethyl-3-(2-(2-methylpropoxy)phenoxy)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloropropyl(diethyl)amine | HCID 66918 | — |
| 反応物 | 2-Isobutoxyphenol | HCID 691161 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Propanamine, N,N-diethyl-3-(2-(2-methylpropoxy)phenoxy)- | HCID 3042675 | — |
反応手順
The compound was prepared as directed in Example 1, using sodium (1.15 g; 50 mole), o-isobutoxyphenol (8.30 g; 50 mmole) and 3-diethylaminopropylchloride (7.50 g; 50 mmole) in 150 ml of ethanol. Yield 8.85 g (63%) of product, boiling at 104°-106° C under a pressure of 0.003 mm Hg, nD25 : 1.4914.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04073917 |
| 出典データセット | uspto-grants-1978_02 |
| ORD ID | ord-8a710dbec9124050b1ba79f771d13d40 |
| 出典メモ | uspto-grants-1978_02 |