HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178422819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178422820 | HCID 178422820 | — |
| Product | HCID 178422819 | HCID 178422819 | — |
Reaction Steps
A suspension of 2.5 g of N2 -(7-methyl-2-naphthalenesulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry diethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry diethyl ether to give N2 -(7-methyl-2-naphthalenesulfonyl)-L-arginyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04073914 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-acb29ca062424e809503929cf98b4ef8 |
| Source note | uspto-grants-1978_02 |