HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-(2-propyl-5-thiazolyl)2,4-pentadienoate → Ethyl 2-propyl-5-thiazole-pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-(2-propyl-5-thiazolyl)2,4-pentadienoate | HCID 54337588 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2-propyl-5-thiazole-pentanoate | HCID 20369849 | 90.5% |
Reaction Steps
Hydrogen was passed through a mixture of 25 g of ethyl 5-(n-propyl-5-thiazolyl)-2,4-pentadienoate, 250 ml of ethanol and 12.5 g of activated carbon containing 10% palladium with stirring for 2 hours and the mixture was filtered and the filter was washed with ethanol. The filtrate was evaporated to dryness under reduced pressure to obtain 23 g of raw ethyl 2-propyl-5-thiazole-pentanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04073919 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-b84e57b553794420912ee8e188156504 |
| Source note | uspto-grants-1978_02 |