Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Malonic Acid → Diethylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Malonic Acid | HCID 867 | — |
| 반응물 | Tetraethylmethylenediamine | HCID 66020 | — |
| 생성물 | Diethylamine | HCID 8021 | — |
| 생성물 | Tetraethylmethylenediamine | HCID 66020 | — |
반응 단계
Malonic acid (5.2g) was added in portions to bis-diethylamino-methane (24g), cooled in ice and stirred manually. A violent reaction took place and the mixture became viscous. Evaportion of the excess bis-diethylamino-methane and diethylamine gave a syrup which was repeatedly recrystallised from acetone to give colourless crystals of 2-diethylaminomethylacrylic acid (5.9g, 76% melting point 121 to 3° C).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04074051 |
| 출처 데이터셋 | uspto-grants-1978_02 |
| ORD ID | ord-cb4386135d6b41cc90b1f80391186a1b |
| 출처 메모 | uspto-grants-1978_02 |