HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → 3-Amino-3-(benzylethylamino)-2-cyanopropenenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 3-Phenylpropylamine | HCID 16259 | — |
| Reactant | Potassium Tricyanomethanide | HCID 10964525 | — |
| Product | 3-Amino-3-(benzylethylamino)-2-cyanopropenenitrile | HCID 86735483 | 70.8% |
Reaction Steps
In a similar manner 27.4 g of benzylethylamine and 13 ml (19.2 g) of methanesulfonic acid were allowed to react. The resulting salt was treated with 25.8 g of potassium tricyanomethanide to yield an additional 32 g of 3-amino-3-(benzylethylamino)-2-cyanopropenenitrile, mp 165°-167°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075001 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-82ef75bc3454485e9b72b15cd1181c66 |
| Source note | uspto-grants-1978_02 |