HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl hydroperoxide → HCID 20367911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 62204-09-5 | HCID 23344794 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20367911 | HCID 20367911 | — |
Reaction Steps
The 2-t-butylazo-2-(t-butylperoxy)-4,4-dimethylpentane was prepared in 78% crude yield from 3.36 grams (.02moles) of 2-t-butylazo-2-chloro-4,4-dimethylpentane, 2.77 grams (.0277 moles) of 90% t-butyl hydroperoxide and 2.0 grams (.025 moles) of 50% NaOH in 20 ml. of methanol. The procedure was the same as that described in Example X.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075199 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-b5ec473fe6b54fbab4f1327eeba147c5 |
| Source note | uspto-grants-1978_02 |