HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thieno(3,2-c)pyridine → Thieno(3,2-c)pyridinium, 5-(o-methoxyphenacyl)-, bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thieno(3,2-c)pyridine | HCID 67500 | — |
| Reactant | Bromomethyl 2-methoxyphenyl ketone | HCID 123440 | — |
| Product | Thieno(3,2-c)pyridinium, 5-(o-methoxyphenacyl)-, bromide | HCID 3041315 | 80.7% |
Reaction Steps
Reaction of thieno[3,2-c]pyridine (13.5 g) with orthomethoxy-phenacyl bromide (21.3 g) according to the procedure of Example 1 gives white crystals (27.34 g) having a melting point (Koefler block) of 258°-260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075215 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-c6a18bb378654af799f130166a78cb4e |
| Source note | uspto-grants-1978_02 |