HCID 20368524, compound → HCID 20368525, compound
Reaction equation
[C:1]1([CH:7]([CH:13]([N:15]([CH3:17])[CH3:16])[CH3:14])[C:8](OCC)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[C:1]1([CH:7]([CH:13]([N:15]([CH3:17])[CH3:16])[CH3:14])[CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
The title compound is prepared according to the procedure of Example 2, from ethyl 2-phenyl-3-dimethylaminobutyrate and lithium aluminum hydride. B.p. 126°-129° C/0.2 mm Hg.
Sources & evidence
- ORD record
- ord-6dae61f868574d47b5581ae7b7406f11
- Source dataset
- uspto-grants-1978_02
- Patent number
- US04075241
Reaction notes
Loading…