HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentabromotoluene → HCID 21330845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentabromotoluene | HCID 6906 | — |
| Reactant | Tetrabromo-o-chlorotoluene | HCID 38294 | — |
| Reactant | HCID 161932 | HCID 161932 | — |
| Product | HCID 21330845 | HCID 21330845 | — |
Reaction Steps
When 2,3,4,5-tetrabromo-6-chlorotoluene, mp 268°-269°, was substituted for pentabromotoluene in Example 7 and the resultant dioxonium compound was hydrolyzed according to the procedure of Example 35 an essentially quantitative yield of the title compound was obtained. The structure of the novel high melting compound was confirmed by infrared and nuclear magnetic resonance spectroscopy as well as by elemental analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075238 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-1fa584f8504649e28f18330360ebeff1 |
| Source note | uspto-grants-1978_02 |