Phosgene → HCID 20368607, compound

HRID 616675Notes

Reaction equation

HRID 616675 reaction equation
C(N=NC(SCCO)(C)C)(C)(C)C.C(Cl)(Cl)=O.[Cl:18][C:19]([O:21][CH2:22][CH2:23][S:24][C:25]([N:31]=[N:32][C:33]([CH3:36])([CH3:35])[CH3:34])([CH3:30])[CH2:26]C(C)C)=[O:20]>>[Cl:18][C:19]([O:21][CH2:22][CH2:23][S:24][C:25]([N:31]=[N:32][C:33]([CH3:36])([CH3:35])[CH3:34])([CH3:30])[CH3:26])=[O:20]

Participants

4

Reactant 3

HCID 6371PhosgeneHCID 20368589HCID 20368589, compoundHCID 2036859157909-39-4

Product 1

HCID 20368607HCID 20368607, compound

Procedure

4-t-Butylazo-4-methyl-3-thiapentyl chloroformate was prepared from 2-t-butylazo-2-(β-hydroxyethylthio)propane and phosgene using the procedure described for the synthesis of 4-t-butylazo-4,6-dimethyl-3-thiaheptyl chloroformate in Example VIb.

Sources & evidence

ORD record
ord-ac4b4fa7ab3f4007a405d26f161bafd4
Source dataset
uspto-grants-1978_02
Patent number
US04075286

Reaction notes

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