HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20300276, compound → HCID 20300267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20300276 | HCID 20300276 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 20300267 | HCID 20300267 | 53% |
Reaction Steps
2-Acetamido-5,6-dihydro-s-triazolo[5,1-a]isoquinoline is reduced with lithium aluminum hydride at 0°-10° C in dimethoxyethane. Yield 53%, m.p. 100°-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075341 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-f667c802b31d4a969b502c31a1043d1a |
| Source note | uspto-grants-1978_02 |