Phenyl isocyanate → HCID 20366859, compound

HRID 616901Notes

Reaction equation

[NH:1]([CH:8]1[CH2:17][CH:16]2[N:11]([CH2:12][CH2:13][C:14]3[CH:21]=[C:20]([O:22][CH3:23])[C:19]([O:24][CH3:25])=[CH:18][C:15]=32)[CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:26]1([N:32]=[C:33]=[O:34])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[CH3:23][O:22][C:20]1[C:19]([O:24][CH3:25])=[CH:18][C:15]2[CH:16]3[N:11]([CH2:12][CH2:13][C:14]=2[CH:21]=1)[CH2:10][CH2:9][CH:8]([N:1]([C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[C:33]([NH:32][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)=[O:34])[CH2:17]3

Participants

Reactant 2

HCID 7672Phenyl isocyanate

HCID 20366868HCID 20366868, compound

Product 1

HCID 20366859HCID 20366859, compound

Procedure

By a procedure analogous to that of Example 1, 2-anilino-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2H-benzo[a]quinolizine (U.S. Pat. No. 3,634,431) is reacted with phenyl isocyanate to give the title compound.

Sources & evidence

ORD record: ord-d6b6114656ae427a931840e4af058d34
Source dataset: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04076820

Reaction notes

Loading…