4-Methylphenyl isocyanate → HCID 20366874, compound

HRID 616904Notes

Reaction equation

HRID 616904 reaction equation
[NH2:1][CH:2]1[CH2:11][CH:10]2[N:5]([CH2:6][CH2:7][C:8]3[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=32)[CH2:4][CH2:3]1.[CH3:16][C:17]1[CH:22]=[CH:21][C:20]([N:23]=[C:24]=[O:25])=[CH:19][CH:18]=1>>[CH2:11]1[CH:10]2[N:5]([CH2:6][CH2:7][C:8]3[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=32)[CH2:4][CH2:3][CH:2]1[NH:1][C:24]([NH:23][C:20]1[CH:21]=[CH:22][C:17]([CH3:16])=[CH:18][CH:19]=1)=[O:25]

Participants

3

Reactant 2

HCID 693254-Methylphenyl isocyanateHCID 129401711,3,4,6,7,11b-Hexahydro-2H-pyrido[2,1-a]isoquinolin-2-amine

Product 1

HCID 20366874HCID 20366874, compound

Procedure

By a procedure analogous to that of Example 1, 2-amino-1,3,4,6,7,11b-hexahydro-2H-benzo[a]quinolizine is reacted with p-methylphenyl isocyanate to give the title compound.

Sources & evidence

ORD record
ord-e3e40bbb80844d26a6f4e911a956fbf3
Source dataset
uspto-grants-1978_02
Patent number
US04076820

Reaction notes

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