HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl alcohol → HCID 135737571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl alcohol | HCID 7859 | — |
| Reactant | HCID 178514316 | HCID 178514316 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 135737571 | HCID 135737571 | — |
Reaction Steps
2.0 g (0.0088 mole) of 7-(trifluoromethyl)-3-diazooxindole and 10.2 g (0.176 mole or 20 equivalents) of 97% propargyl alcohol are refluxed under N2 for 4 hours, cooled, diluted with ether (200 ml) and stirred for 30 minutes. The light pink solid that forms is filtered off. Yield: 1.3 g; 52.2% crude yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04076818 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-55379147f7f94bb4a939f6097079af70 |
| Source note | uspto-grants-1978_02 |