Aniline → N-Phenyldodecanamide

HRID 616986Notes

Reaction equation

HRID 616986 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:8](Cl)(=[O:20])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>>[C:8]([NH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)(=[O:20])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

3

Reactant 2

HCID 6115AnilineHCID 8166Dodecanoyl chloride

Product 1

HCID 94794N-PhenyldodecanamideYield 84%

Procedure

N-dodecanoylaminobenzene was prepared by acylation of aminobenzene with lauroyl chloride by a procedure similar to that of Example 1(a). After crystallization from hexane, a yield of 84% of white crystalline plates m.p. 76.3°-76.8° C. was obtained.

Workup

  1. customAfter crystallization from hexane
  2. customa yield of 84% of white crystalline plates m.p. 76.3°-76.8° C. was obtained

Sources & evidence

ORD record
ord-a84670e396a44fe680e6029cf69ab4af
Source dataset
uspto-grants-1978_02
Patent number
US04076849

Reaction notes

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