tert-Butyl ethyl(2-hydroxyethyl)carbamate → HCID 86663816, compound

HRID 61702Notes

Reaction equation

HRID 61702 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[C:17](=[O:18])[C:16]3[C:15]4[C:10](=[CH:11][C:12]([C:19]#[N:20])=[CH:13][CH:14]=4)[NH:9][C:8]=3[C:7]([CH3:22])([CH3:21])[C:6]=2[CH:23]=1.[C:24]([O:28][C:29](=[O:36])[N:30]([CH2:34][CH3:35])[CH2:31][CH2:32]O)([CH3:27])([CH3:26])[CH3:25]>>[C:24]([O:28][C:29](=[O:36])[N:30]([CH2:31][CH2:32][O:1][C:2]1[CH:3]=[CH:4][C:5]2[C:17](=[O:18])[C:16]3[C:15]4[C:10](=[CH:11][C:12]([C:19]#[N:20])=[CH:13][CH:14]=4)[NH:9][C:8]=3[C:7]([CH3:21])([CH3:22])[C:6]=2[CH:23]=1)[CH2:34][CH3:35])([CH3:26])([CH3:27])[CH3:25]

Participants

3

Reactant 2

HCID 14925142tert-Butyl ethyl(2-hydroxyethyl)carbamateHCID 668338618-Hydroxy-6,6-dimethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

Product 1

HCID 86663816HCID 86663816, compound

Procedure

Under the same conditions as the method for synthesizing Compound A7-1, the title compound was prepared from Compound A6 and ethyl-(2-hydroxy-ethyl)-carbamic acid tert-butyl ester.

Workup

  1. customUnder the same conditions as the method for synthesizing Compound A7-1

Sources & evidence

ORD record
ord-4458eb8101184b60b0484d81cf8a3678
Source dataset
uspto-grants-2016_09
Patent number
US09440922B2

Reaction notes

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