beta-Aminobeta-ethoxyacrylic acid ethyl ester → HCID 20367266, compound

HRID 617030Notes

Reaction equation

HRID 617030 reaction equation
C([O:3][C:4](=O)[CH:5]=[C:6]([NH2:10])OCC)C.[CH2:12]1[O:23][C:22]2[CH:21]=[CH:20][C:16]([CH2:17][NH:18][NH2:19])=[CH:15][C:14]=2[O:13]1>>[NH2:10][C:6]1[NH:19][N:18]([CH2:17][C:16]2[CH:20]=[CH:21][C:22]3[O:23][CH2:12][O:13][C:14]=3[CH:15]=2)[C:4](=[O:3])[CH:5]=1

Participants

3

Reactant 2

HCID 278451beta-Aminobeta-ethoxyacrylic acid ethyl esterHCID 416803[(2H-1,3-Benzodioxol-5-yl)methyl]hydrazine

Product 1

HCID 20367266HCID 20367266, compound

Procedure

From 17.5 g of β-amino-β-ethoxyacrylic acid ethyl ester and 16.6 g of 3,4-methylenedioxybenzylhydrazine, analogously to the procedure described in Example 1. 12.1 g of the compound identified above, as colorless crystals of melting point 218°, corresponding to 52% of theory, are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-413604a12f704a1588753cf06ad9e0be
Source dataset
uspto-grants-1978_02
Patent number
US04076943

Reaction notes

Loading…