Hydrochloric Acid → HCID 21309685, compound

Participants

Reaction Steps

The compound from step 47b was treated with HCl in ether according to Example 14c to afford the title compound. MS (DCI/NH3) m/e: 223 (M+H)+. 1H NMR (D2O, 300 MHz) δ: 8.61 (m, 1H), 8.43 (d, 1H, J=5.32 Hz), 7.91 (m, 1H), 7.74 dd, 1H, J=5.34, 8.1 Hz), 4.61-4.53 (m, 2H), 4.14 (m, 1H), 3.98 (m, 1H), 3.81 (m, 1H), 3.30 (s, 3H), 3.22 (m, 1H), 2.96 (s, 3H), 2.37 (m, 1H), 2.01 (m, 1H). Anal. Calc. for C12H20N2O2Cl2 : C, 48.82; H, 6.82; N, 9.49; Found C, 48.56; H, 6.88; N, 9.43.

Provenance & Evidence