3-Mercaptopropionic Acid → HCID 66833819, compound

HRID 61750Notes

Reaction equation

HRID 61750 reaction equation
[C:1]([C:3]1[CH:15]=[C:14]2[C:6]([C:7]3[C:8](=[O:30])[C:9]4[CH:21]=[CH:20][C:19](OS(C(F)(F)F)(=O)=O)=[CH:18][C:10]=4[C:11]([CH3:17])([CH3:16])[C:12]=3[NH:13]2)=[CH:5][CH:4]=1)#[N:2].[SH:31][CH2:32][CH2:33][C:34]([OH:36])=[O:35]>>[C:1]([C:3]1[CH:15]=[C:14]2[C:6]([C:7]3[C:8](=[O:30])[C:9]4[CH:21]=[CH:20][C:19]([S:31][CH2:32][CH2:33][C:34]([OH:36])=[O:35])=[CH:18][C:10]=4[C:11]([CH3:17])([CH3:16])[C:12]=3[NH:13]2)=[CH:5][CH:4]=1)#[N:2]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 86663817Trifluoro-methanesulfonic acid 3-cyano-6,6-dimethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazol-8-yl ester

Product 1

HCID 66833819HCID 66833819, compound

Procedure

Under the same conditions as the method for synthesizing Compound B2-17, the title compound was prepared from Compound B1 and 3-mercaptopropionic acid.

Sources & evidence

ORD record
ord-0788d0312e4c490e96484198ec49aaf0
Source dataset
uspto-grants-2016_09
Patent number
US09440922B2

Reaction notes

Loading…