1,3-Benzodioxole-5-ethanamine → HCID 23289801, compound

HRID 617562Notes

Reaction equation

HRID 617562 reaction equation
[CH2:1]1[O:12][C:11]2[CH:10]=[CH:9][C:5]([CH2:6][CH2:7][NH2:8])=[CH:4][C:3]=2[O:2]1.[CH3:13][O:14][C:15](=[O:34])[C:16]1[CH:21]=[CH:20][C:19]([C:22]2[N:23]=[C:24](Cl)[C:25]3[C:30]([CH3:31])=[C:29]([CH3:32])[S:28][C:26]=3[N:27]=2)=[CH:18][CH:17]=1>>[CH3:13][O:14][C:15](=[O:34])[C:16]1[CH:17]=[CH:18][C:19]([C:22]2[N:23]=[C:24]([NH:8][CH2:7][CH2:6][C:5]3[CH:9]=[CH:10][C:11]4[O:12][CH2:1][O:2][C:3]=4[CH:4]=3)[C:25]3[C:30]([CH3:31])=[C:29]([CH3:32])[S:28][C:26]=3[N:27]=2)=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 738741,3-Benzodioxole-5-ethanamineHCID 23289650HCID 23289650, compound

Product 1

HCID 23289801HCID 23289801, compound

Procedure

The reaction procedure as above wherein 3,4-methylenedioxyphenethylamine is reacted with 4-(4-chloro-5,6-dimethyl-thieno-[2,3-d]-pyrimidin-2-yl)-benzoic acid methylester yields 4-[4-(3,4-methylenedioxyphenethylamino)-5,6-dimethyl-thieno-[2,3-d]-pyrimidin-2-yl]-benzoic acid methylester.

Sources & evidence

ORD record
ord-9346c9e90295434e9b32147c1b97bae9
Source dataset
uspto-grants-1999_09
Patent number
US05948911

Reaction notes

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