HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22618714, compound → HCID 22618819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22618714 | HCID 22618714 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22618819 | HCID 22618819 | 61.2% |
Reaction Steps
To a solution of 4-(2-(2-benzyloxyphenyl)ethyl)-4-methyl-2-oxazolidinone (4.60 g) in ethanol (200 ml), 10% palladium-carbon (0.60 g) was added and the mixture was subjected to catalytic reduction at room temperature for 6 hours. Catalyst was filtered off form the reaction solution and the solvent was distilled away under reduced pressure. The residue was crystallized from ether-isopropyl ether to give the subject compound (2.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948820 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-e7fd910a17d54e1dba9abeb990d2551b |
| Source note | uspto-grants-1999_09 |