HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 3-methylbenzimidate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Tolunitrile | HCID 12104 | — |
| Product | Ethyl 3-methylbenzimidate hydrochloride | HCID 21938086 | — |
Reaction Steps
Ethyl 3-methylbenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, m-tolunitrile (25.2 g, 0.215 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 41.7 g (97%) of the target compound as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948785 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-472e9956c224470ca9bd5bd552bcd52d |
| Source note | uspto-grants-1999_09 |