HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 3,5-dinitrobenzimidate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzonitrile, 3,5-dinitro- | HCID 20062 | — |
| Product | Ethyl 3,5-dinitrobenzimidate hydrochloride | HCID 12509993 | — |
Reaction Steps
Ethyl 3,5-dinitrobenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, 3,5-dinitrobenzonitrile (25.2 g, 0.130 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 34.5 g (96%) of the target compound as pale-brown crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948785 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-ed5b6405628f482c8086e29f0e682231 |
| Source note | uspto-grants-1999_09 |