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HRID61775

反应详情

EQUATION

反应方程式

HRID 61775 的结构方程式

REACTANTS

反应物

2
结构：C[n+]1ccn(S(=O)(=O)n2ccnc2)c1
HCID11728150

未命名化合物

结构：CC1(C)c2cc(C3CCNCC3)ccc2C(=O)c2c1[nH]c1cc(C#N)ccc21
HCID66833995

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)c2cc(C3CCN(S(=O)(=O)n4ccnc4)CC3)ccc2C(=O)c2c1[nH]c1cc(C#N)ccc21
HCID66834132

未命名化合物

收率 22.2%

PROCEDURE

实验过程

According to the method disclosed in Journal of Organic Chemistry, 2003, page 115, 6,6-dimethyl-11-oxo-8-piperidin-4-yl-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile (Compound B3-13-2, 10 mg, 0.027 mmol) was reacted with 3-(imidazole-1-sulfonyl)-1-methyl-3H-imidazol-1-ium (19 mg, 2 eq.). After removing the solvent, the residues were purified by liquid chromatography to obtain the title compound (3 mg).

WORKUP

后处理

  1. customAfter removing the solvent
  2. customthe residues were purified by liquid chromatography