HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21849941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | HCID 21849919 | HCID 21849919 | — |
| Product | HCID 21849941 | HCID 21849941 | 53% |
Reaction Steps
Subsequently, 20 ml of ethanol was added to 540 mg (2.1 mmol) of 7-(2-aminophenyl)benz[g]indole and 260 mg (2.5 mmol) of ethyl glyoxylate (polymeric) and the obtained mixture was heated under reflux for 8 hours. After distilling off the solvent, the residue was purified by silica gel column chromatography to thereby give 380 mg (yield: 53%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952335 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-a43ab31f441f45d180499f3e08e8fb9c |
| Source note | uspto-grants-1999_09 |