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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 617810Generated: October 31, 2026

Ethanol → HCID 21849941, compound

https://huagongshe.com/reaction/617810

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantEthyl oxoacetateHCID 70211—
ReactantHCID 21849919HCID 21849919—
ProductHCID 21849941HCID 2184994153%

Reaction Steps

Subsequently, 20 ml of ethanol was added to 540 mg (2.1 mmol) of 7-(2-aminophenyl)benz[g]indole and 260 mg (2.5 mmol) of ethyl glyoxylate (polymeric) and the obtained mixture was heated under reflux for 8 hours. After distilling off the solvent, the residue was purified by silica gel column chromatography to thereby give 380 mg (yield: 53%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05952335
Source datasetuspto-grants-1999_09
ORD IDord-a43ab31f441f45d180499f3e08e8fb9c
Source noteuspto-grants-1999_09