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Triphenylphosphine → Decyltriphenylphosphonium bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triphenylphosphine | HCID 11776 | — |
| 反応物 | Decane bromide | HCID 18759729 | — |
| 生成物 | Decyltriphenylphosphonium bromide | HCID 3084561 | — |
反応手順
Decane bromide (7.0 g) and 10 g of triphenylphosphine were stirred at 120° C. under a nitrogen atmosphere for 8 hours. The mixture was recrystallized from acetone-ether to give 14.4 g of colorless, crystalline decyltriphenylphosphonium bromide. IRνmax (CHCl3): 2920, 2850, 1440, 1120, 1000, 680 cm-1
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952316 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-3075facca349438ba2ee1659417732c0 |
| 出典メモ | uspto-grants-1999_09 |