HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-(1,2-dihydroxy-4-octadecenyl)-1,3-propanediol → 2-Amino-2-(1,2-dihydroxyoctadecyl)-1,3-propanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-(1,2-dihydroxy-4-octadecenyl)-1,3-propanediol | HCID 53863801 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-2-(1,2-dihydroxyoctadecyl)-1,3-propanediol | HCID 21849353 | 50.2% |
Reaction Steps
2-Amino-2-(1,2-dihydroxy-4-octadecenyl)-1,3-propanediol (68.0 mg) was dissolved in 14 ml of methanol and 6.8 mg of 5% palladium-carbon was added thereto. The catalytic reduction was conducted at ordinary temperature and at atmospheric pressure day and night. After the reaction, the catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 34.3 mg of the subject compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952316 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-dda39b44ffd84448bec54c3cc1259b31 |
| Source note | uspto-grants-1999_09 |