HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53792649, compound → HCID 54205831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53792649 | HCID 53792649 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54205831 | HCID 54205831 | 92.5% |
Reaction Steps
10% Palladium carbon (0.1 g) was added to a solution (30 ml) of 2-acetamido-2-[2-{4-(7-octenyloxy)phenyl}ethyl]-1,3-propanediol diacetate (1.27 g) in ethanol and the mixture was stirred at ordinary temperature and at atmospheric pressure for 6 hours under a hydrogen atmosphere. The catalyst was filtered off and the filtrate was concentrated. The residue was collected by filtration to give the subject compound (1.18 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952316 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-0a5dde6b043b4ac5a224cfd84b19cfa5 |
| Source note | uspto-grants-1999_09 |