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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 617908Generated: November 1, 2026

Hydrochloric Acid → HCID 86754155, compound

https://huagongshe.com/reaction/617908

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantEthanolHCID 702—
ReactantHCID 10547108HCID 10547108—
ProductHCID 86754155HCID 86754155—

Reaction Conditions

Temperature60 °C

Reaction Steps

HCl gas was rapidly bubbled through a suspension of acid 9-3 (4.0 g, 10.81 mmol) in EtOH (50 ml) at 0° C. for 10 minutes. The cooling bath was removed and the reaction was heated to 60° C. After 18 h, the reaction was concentrated to provide ester 9-4 as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05952341
Source datasetuspto-grants-1999_09
ORD IDord-89bcfcdde8a446e6961244ef7b1b8f41
Source noteuspto-grants-1999_09