HRID617988
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound was prepared using 0.30 g of 6-(2-bromo-6-chloro-phenyl)-pyrido[2,3-d]pyrimidine-2,7-diamine from Example 104 and 0.105 mL of tert-butyl isocyanate according to Example 2. The product was purified by MPLC eluting with 1:1 CHCl3 :EtOAc; mp 314° C. (dec); MS(CI).
WORKUP
后处理
- customThe product was purified by MPLC
- washeluting with 1:1 CHCl3