HRID618081

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID67789

4-Fluorothiophenol

C6H5FS

HCID3685732

2-bromo-1-(3,4,5-trimethoxyphenyl)ethanone

C11H13BrO4

PRODUCTS

生成物

HCID21850267

未命名化合物

收率 125%

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 13 was repeated using 4-fluorothiophenol (0.82 g) and 2-bromo-3',4',5'-trimethoxyacetophenone (Compound XIa, 1.54 g) obtained in Reference Example 1 to give 2-(4-fluorophenylthio)-3',4',5'-trimethoxyacetophenone (Compound IX-11, 2.24 g).

WORKUP

后处理

customobtained in Reference Example 1