HRID618083

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7291

1-Thioglycerol

C3H8O2S

HCID3685732

2-bromo-1-(3,4,5-trimethoxyphenyl)ethanone

C11H13BrO4

PRODUCTS

生成物

HCID21850159

未命名化合物

收率 94.8%

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 13 was repeated using 1-mercapto-2,3-propanediol (12.25 g) and 2-bromo-3',4',5'-trimethoxyacetophenone (Compound XIa, 16.39 g) obtained in Reference Example 1 to give 2-(2,3-dihydroxypropylthio)-3',4',5'-trimethoxyacetophenone (Compound IX-13, 17.00 g).

WORKUP

后处理

customobtained in Reference Example 1