Benzenesulfonyl chloride → HCID 15432611, compound

HRID 618096Notes

Reaction equation

HRID 618096 reaction equation
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3](/[CH:10]=[CH:11]/[C:12]([C:14]2[CH:19]=[C:18]([O:20][CH3:21])[C:17]([O:22][CH3:23])=[C:16]([O:24][CH3:25])[CH:15]=2)=[O:13])=[CH:2]1.[C:26]1([S:32](Cl)(=[O:34])=[O:33])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[C:26]1([S:32]([N:1]2[C:9]3[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=3)[C:3](/[CH:10]=[CH:11]/[C:12]([C:14]3[CH:19]=[C:18]([O:20][CH3:21])[C:17]([O:22][CH3:23])=[C:16]([O:24][CH3:25])[CH:15]=3)=[O:13])=[CH:2]2)(=[O:34])=[O:33])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 7369Benzenesulfonyl chlorideHCID 9927763170488-48-9

Product 1

HCID 15432611HCID 15432611, compoundYield 85.8%

Procedure

Substantially the same procedure as in Example 9 was repeated using Compound 1 (337.4 mg) obtained in Example 1 and benzenesulfonyl chloride (176.6 mg) to give Compound 10 (409.9 mg).

Sources & evidence

ORD record
ord-6ea9fee40cf440f0856f8382273fa6f8
Source dataset
uspto-grants-1999_09
Patent number
US05952355

Reaction notes

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