HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 86754481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 86754482 | HCID 86754482 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86754481 | HCID 86754481 | — |
Reaction Steps
Ester 9-3 (44 mg, 0.1 1 mmol) was dissolved in 1.1 mL THF, then 1 N LiOH (0.28 mL, 0.28 mmol) was added. After stirring overnight the reaction mixture was loaded directly onto a flash chromatography column (silica, eluting with 7:20:1:1 EtOAc/EtOH/H2O/NH4OH) providing 9-4 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952306 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-bc83cf3bf02346dabe1150fc1562adf0 |
| Source note | uspto-grants-1999_09 |