HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methanesulfonyl-6-hydroxymethylindole → 5-Bromomethyl-1-chloro-2-methyl-3-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methanesulfonyl-6-hydroxymethylindole | HCID 18789614 | — |
| Reactant | N-methanesulfonyl-6-bromomethylindole | HCID 18789641 | — |
| Reactant | (3-Chloro-4-methyl-5-nitrophenyl)methanol | HCID 18789738 | — |
| Product | 5-Bromomethyl-1-chloro-2-methyl-3-nitrobenzene | HCID 18789673 | — |
Reaction Steps
5-Bromomethyl-1-chloro-2-methyl-3-nitrobenzene was prepared from (3-chloro-4-methyl-5-nitrophenyl)methanol in a manner similar to that described in Example 10 for the preparation of N-methanesulfonyl-6-bromomethylindole from N-methanesulfonyl-6-hyroxymethyl indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952362 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-43b921327faf4ed4a52e62a784e02be2 |
| Source note | uspto-grants-1999_09 |