HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 5-bromothiophene-2-carboxylate → HCID 22000374, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 5-bromothiophene-2-carboxylate | HCID 605713 | — |
| Edukt | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| Produkt | HCID 22000374 | HCID 22000374 | 65,5% |
Reaktionsschritte
Following the procedure of Example 1(c), but reacting 1.5 g (3.6 mmol) of 7-(l-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 400 mg (1.8 mmol) of methyl 5-bromo-2-thiophenecarboxylate, 600 mg (65%) of the expected compound were obtained, which compound had a melting point of 170°-1° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05952382 |
| Quelldatensatz | uspto-grants-1999_09 |
| ORD ID | ord-04286c2faeac4fcbae01bd8dac08d730 |
| Quellennotiz | uspto-grants-1999_09 |