化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 4-iodobenzoate → Methyl 4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 4-iodobenzoate | HCID 69273 | — |
| 反応物 | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| 生成物 | Methyl 4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate | HCID 22000300 | 33.5% |
反応手順
Following the procedure of Example 1(c), but reacting 1.5 g (3.6 mmol) of 7-(1-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 500 mg (1.9 mmol) of methyl 4-iodobenzoate, 320 mg (33%) of the compound were obtained, which compound had a melting point of 170°-3° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952382 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-44fbc64ee8794188a119649a305c5468 |
| 出典メモ | uspto-grants-1999_09 |