HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodosalicylate → HCID 22000377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodosalicylate | HCID 11380407 | — |
| Reactant | HCID 22000338 | HCID 22000338 | — |
| Product | HCID 22000377 | HCID 22000377 | 78% |
Reaction Steps
Following the procedure of Example 1(c), but reacting 560 mg (1.41 mmol) of 7-(1-adamantyl)-6-(4-fluorobenzyl)oxy-2-naphthylboronic acid with 330 mg (1.17 mmol) of methyl 2-hydroxy-4-iodobenzoate, 490 mg (78%) of the expected ester were obtained, which ester had a melting point of 189°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952382 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-07890b4d9c4e463597d5653818d4e68e |
| Source note | uspto-grants-1999_09 |