HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodosalicylate → HCID 70231312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodosalicylate | HCID 11380407 | — |
| Reactant | HCID 56991437 | HCID 56991437 | — |
| Product | HCID 70231312 | HCID 70231312 | 81.3% |
Reaction Steps
Following the procedure of Example 1(c), but reacting 2.25 g (5.5 mmol) of 7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthylboronic acid with 1.39 g (5 mmol) of methyl 2-hydroxy-4-iodobenzoate, 2.1 g (81%) of the expected ester were obtained, which ester had a melting point of 101°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952382 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-ad089fa751094caa81088ab2dd0f5c43 |
| Source note | uspto-grants-1999_09 |