HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromohexanamide → Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromohexanamide | HCID 321974 | — |
| Reactant | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| Product | Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate | HCID 21850744 | 66% |
Reaction Steps
Following the procedure of Example 12(a), but reacting 640 mg (1.55 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 450 mg (2.32 mmol) of 6-bromohexanamide, 520 mg (65%) of the expected compound were obtained, which compound had a melting point of 209°-10° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952382 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-55058d0f2c0a4a00b492fdcfcf9a0cb5 |
| Source note | uspto-grants-1999_09 |