HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 22000347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 70231423 | HCID 70231423 | — |
| Product | HCID 22000347 | HCID 22000347 | 14% |
Reaction Steps
Following the procedure of Example 12(a), but reacting 870 mg (1.7 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxyhexyloxy-2-naphthyl]benzoate with 160 μl (1.7 mmol) of dimethyl sulphate, 100 mg (14%) of the expected compound were obtained, which compound had a melting point of 141°-3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952382 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-5b80033358bf4e65bdd8153517f55065 |
| Source note | uspto-grants-1999_09 |