Methanol → Z-Gln-ome

Participants

Role	Name	HCID	Charge
Reactant	Methanol	HCID 887	—
Reactant	Sulfuryl chloride	HCID 24648	—
Reactant	L-Glutamine, N2-[(phenylmethoxy)carbonyl]-	HCID 75855	—
Product	Z-Gln-ome	HCID 7020255	—

Reaction Steps

Sulphuryl chloride (1 g) was added to a stirred mixture of N-benzyloxycarbonyl-L-glutamine (100 g) and methanol (1200 ml) and the mixture was stirred at ambient temperature for 24 hours. The mixture was evaporated to give N-benzyloxycarbonyl-L-glutamine methyl ester (105 g).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05955463
Source dataset	uspto-grants-1999_09
ORD ID	ord-7c388e813ccc4a57ab2a1f330e68813f
Source note	uspto-grants-1999_09