Acetonitrile → HCID 70100273, compound

Participants

Reaction Conditions

Reaction Steps

Disolve the product of Example 9 (1 equivalent) in an inert anhydrous solvent such as CH3CN, benzene or toluene and add Et3N (2 equivalents). Cool the solution to 0° C. and add N-methylsulfamoyl chloride (1.2 equivalents) [prepared as described in: J. A. Kloek and K. L. Leschinsky, J. Org. Chem., 41 (25) (1976), p. 4028-4029]. Stir the mixture at 0° C. to 25° C. for 3 h, extract, filter and evaporate to give the title compound.

Provenance & Evidence