HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 21845224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phenyl phosphorus dichloride | HCID 12573 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | HCID 86752773 | HCID 86752773 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21845224 | HCID 21845224 | 21% |
Reaction Steps
It is prepared from 4-dodecyloxy-N,N-di(2-hydroxy)ethyl aniline (3.66 g, 10 mmol), pyridine (2 g, 25 mmol), dimethylaminopyridine (0.2 g) and phenylphosphonous dichloride (2.15 g, 11 mmol) in dichloromethane as described for compound 200 to obtain a white solid 1 g (21%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958663 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-d5ca9ba4b8b0435ca1105aa916ca7f89 |
| Source note | uspto-grants-1999_09 |