HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 21845230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phenyl phosphorus dichloride | HCID 12573 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | HCID 54386311 | HCID 54386311 | — |
| Reactant | HCID 86752773 | HCID 86752773 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21845230 | HCID 21845230 | 32% |
Reaction Steps
It is prepared from 4-methoxy-N,N-di(2-hydroxy-3-ethyl-hexyloxy)-propyl aniline (2 g, 4 mmol), pyridine (0.8 g, 10 mmol), dimethylaminopyridine (0.2 g) and phenylphosphonous dichloride (0.8 g, 4 mmol) in dichloromethane as described for compound 200 to obtain a pale yellow liquid 0.8 g (32%) and its isomer 0.85 g (34%, a pale yellow liquid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958663 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-8a0e9ee58ace42ad9f17e85146a6ec77 |
| Source note | uspto-grants-1999_09 |