HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12109159, compound → HCID 12109152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12109159 | HCID 12109159 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178420936 | HCID 178420936 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12109152 | HCID 12109152 | 100.3% |
Reaction Steps
Methyl (R)-4-(1-acetamidoethyl)-3-nitrobenzoate (1 g) was stirred in a stream of hydrogen at room temperature for 3 hours using 10% palladium hydroxide carbon (0.3 g) in a methanol (20 ml) solution. After the reaction, the catalyst was removed by filtration, and the solvent was evaporated under reduced pressure to give 0.89 g of methyl (R)-3-amino-4-(1-acetamidoethyl)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958944 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-e4cbea4c866c4f56a3cc6e734618c5d3 |
| Source note | uspto-grants-1999_09 |