Ethylene carbonate → HCID 21995164, compound

Participants

Reaction Steps

The compound was prepared in a manner analogous to the preparation of the compound of Example 47 from the compound of Example 49 (250 mg, 0.71 mmol), ethylene carbonate (70 mg, 6.78 mmol) and 60% sodium hydride (dispersion in oil) (30 mg, 0.78 mmol) to give the title compound (140 mg) as a yellow solid m.p 145-146°. MS m/z 398 (M+H)+.

Provenance & Evidence