HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70212801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21190117 | HCID 21190117 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70212801 | HCID 70212801 | 99.6% |
Reaction Steps
To a suspension of 500 mg (1.62 mmol) of 1,2-dihydro-3-methyl-1-[3-(methanesulfonamido)propan-1-yl]-1,4,7b-triazacyclopent[cd]inden-2-one in 30 ml of methanol was added 0.18 ml of conc. HCl. The solvent was distilled off to give 557 mg of the desired compound (99.6%, pale yellow crystals), m.p.184.0-185.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958942 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-30a421d3e3314f99a525b889d245f071 |
| Source note | uspto-grants-1999_09 |