HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 136136193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Dodecanoyl chloride | HCID 8166 | — |
| Reactant | HCID 136138660 | HCID 136138660 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 136136193 | HCID 136136193 | — |
Reaction Steps
A mixture of 5.0 g (11.3 mmol) of 2,4-diphenyl-6-(2'-hydroxy-4'-(2"- hydroxycyclohexyloxy)phenyl)-1,3,5-triazine, 5.7 g (26 mmol) of dodecanoyl chloride (Fluka, 98%) and 0.1 g (1.3 mmol) of pyridine in 60 ml of toluene is stirred under nitrogen and kept at 50° C. for 20 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05959008 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-5cb3c55f2f6a40029921621cafaba363 |
| Source note | uspto-grants-1999_09 |